Open Access
 Issue Int. J. Metrol. Qual. Eng. Volume 8, 2017 14 9 https://doi.org/10.1051/ijmqe/2017014 24 May 2017

This is an Open Access article distributed under the terms of the Creative Commons Attribution License (http://creativecommons.org/licenses/by/4.0), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

## 1 Introduction

The guide to the expression of measurement uncertainty (GUM, JCGM 100) and the propagation of distributions by a Monte Carlo method (GUMS1, JCGM 101) are two of the most widely used documents concerning measurement uncertainty evaluation in metrology. Both documents describe three phases: (a) the construction of a measurement model, (b) the assignment of probability distributions to quantities, and (c) a computational phase that specifies the distribution for the quantity of interest. The two approaches described in these two documents agree in the first two phases but employ different computational approaches, with the GUM using linearization to simplify the calculations [1]. The guide to the Expression of Uncertainty in Measurement (GUM) requires, “that the results of a measurement have been corrected for all recognized significant systematic effects and that every effort has been made to identify such effects”, before the issue of evaluating their uncertainty is tackled [2]. GUM provides a framework and procedure for evaluating and expressing measurement uncertainty. GUM procedure has two main limitations. Firstly, the way that the coverage interval is constructed to contain values of the measurand with a stipulated coverage probability is approximate. Secondly, insufficient guidance is given for the multivariate case in which there is more than one measurand [3]. Figure 1 shows the schematic to explain the main idea of GUM which mainly depends on the uncertainty propagations [4].

Monte Carlo Simulation (MCS) is the second method to estimate the uncertainty of measurements, where evaluating the measurement uncertainty by the MCS method can be carried out by establishments of the model equation for the measurand in function of the individual parameters of influence, then selecting the significant sources of uncertainty, identification of the probability density functions corresponding to each source of uncertainty selected, and selecting the number Monte Carlo trials, and finally calculating the M results by applying the equation that was defined for the measurand [5].

MCS process is illustrated in Figure 2a and b in comparison with the propagation of uncertainties used by the GUM.

Figure 2a shows an illustration representing the propagation of uncertainties. In this case, three input quantities are presented x1, x2 and x3 along with their respective uncertainties u(x1), u(x2) and u(x3). As can be noted, only the main moments (expectation and standard deviation) of the input quantities are used in the propagation. In Figure 2b, while propagating density (PDFs), no approximations are made and the whole information contained on the input distributions is propagated to the output [5].

The aims of this present research article are to investigate the differences between GUM and MCS as methods of uncertainty estimation of hardness and to detect the effects of inputs correlation on the uncertainty budget.

 Fig. 1GUM and propagation of uncertainties.
 Fig. 2Schematic to the main idea of MCS.

## 2 Theoretical principle

### 2.1 Uncertainty classifications

To investigate the difference between GUM and MCS, the resultant budget uncertainties of Brinnell and Vickers hardness (HV) measurements were used as an application. For statistical analysis normal PDFs were proposed. The uncertainty estimated from normal distribution is believed to lie in the interval defined by U with a level of confidence of approximately 95%. For normal distribution, μ is the expectation or mean of the distribution, and the shaded areas represent ±1.96 standard uncertainty ustnd about the mean, and ±ustnd, encompasses about 95% of the distribution (see Fig. 3).

Each input source of the uncertainty should be classified as type A or type B where type A evaluation of standard uncertainty is based on any valid statistical method for treating data and can be calculated by the following equations: (1) (2) where Xi is an input quantity whose value is estimated from n independent observations Xi,k of Xi obtained under the same conditions of measurement, and the standard uncertainty u(xi) to be associated with xi is the estimated standard deviation of the mean. For type B standard uncertainty, the evaluation of standard uncertainty is usually based on scientific judgment using all of the relevant information available, that is, the uncertainty is either obtained from an outside source, or obtained from an assumed distribution.

 Fig. 3The normal distribution, and standard deviation with the confidence level.

### 2.2 Uncertainty in measurements with and without correlation

If the functional relationship between the measurand Y and the input quantities X in a measurement process is given by [6]; (3) The function f is used to calculate the output estimates: y, of the measurand; Y, using the estimates of X1, X2, X3, … , XN for the values of the N input quantities. (4)The conventional estimation can be illustrated using a simple equation with y as a continuous function of x1, x2. y is approximated using a polynomial approximation or a 2nd order Taylor's series expansion about the means: (5)where are mean values and Z is the remainder: (6)As the partial derivatives are computed at the mean values they are the same for all i = 1, 2, …, N. All the higher terms are normally neglected at Z = 0, so equation (5) becomes; (7)If f(x1, x2) is a linear function, then the second order partial derivatives in equation (6), are zero, so Z = 0. Both linearity and small uncertainty are prerequisites of conventional method of uncertainty estimation described below. The standard deviations σ(X1), σ(X2) are referred by GUM [7], as the standard uncertainties associated with the input estimates X1, X2. The standard uncertainty in y can be obtained by Taylor equation [8]; (8)This equation gives the uncertainty as a standard deviation irrespective of whether or not the measurements of x1, x2 are independent and of the nature of the probability distribution. In the case of correlated inputs then equation (3) can be written in terms of the correlation coefficient ; (9)

The correlation coefficient can be calculated by the following equation [9]: (10) As a direct consequence of its definition, the correlation coefficient r is restricted to the range ‒1 through zero to +1. When r = 0, the correlation is zero, when r = +1, the correlation is perfect and positive, and when r = −1 the correlation is perfect and negative.

The partial derivatives are called sensitivity coefficients, which give the effects of each input quantity on the final results (or the sensitivity of the output quantity to each input quantity). The term, expanded uncertainty is used in GUM to express the % confidence interval about the measurement result within which the true value of the measurand is believed to lie and is given by: (11) where k is the coverage factor on the basis of the confidence required for the interval, (12)If it was considered that y = x1 + x2 is a linear operation it was reported that there is compatibility between MCS and GUM and it was demonstrated that at correlated or uncorrelated inputs MCS gives identical results as given in equations (5) and (9). The results of y are linear functions in terms of x1 and x2. As the first order partial derivatives are all equal to ±1, the square is equal to unity. The second order partial derivatives are both equal to zero.

To quantify the distribution of the results of Skewness and Kurtosis, where Skewness quantifies how symmetrical the distribution, it can be calculated from the following equation: (13) where

• Positive Skewness indicates a long right tail;

• Negative Skewness indicates a long left tail;

• Zero Skewness indicates a symmetry around the mean.

Kurtosis quantifies whether the shape of the data distribution matches the Gaussian distribution and it can be calculated from the following equation: (14)

• Positive excess Kurtosis indicate flatness (long, fat tails);

• Negative excess Kurtosis indicates peakedness.

### 2.3 Brinell hardness (HB) results

This test is executed by applying a load on a sphere made of a hard material over the surface of the test sample (Fig. 4) [10].

During the test the sphere will penetrate through the sample leaving an indented mark upon unloading. The diameter of this indentation is inversely proportional to the hardness of the material of the sample. The model used for the HB is represented in equation (15) [11]. (15) where F is the applied load (N), D is the indenter diameter (mm) and d is the diameter of the indentation mark (mm).

 Fig. 4Schematic represents the Brinell hardness test.

### 2.4 HV results

HV is a measure of the hardness of a material, calculated from the size of an impression produced under load by a pyramid-shaped diamond indenter (Fig. 5) [12].

During the test the square pyramid indenter will penetrate through the sample leaving an indented mark upon unloading. The two diagonals of this indentation are measured and the mean of them was calculated.

The model used here for the HV is represented in equation (16) [12]. (16) where F is the applied load (kgf), and d is the mean of d1 and d2 of the indentation mark (mm).

 Fig. 5Schematic represents Vickers hardness test.

## 3 Application results

### 3.1 Procedure to estimate the uncertainty of HB

To estimate the uncertainty it is required to detect all the input sources of uncertainty of HB measurements. These sources can be summarized as shown in Figure 6.

After detecting these parameters, measurements were performed and the results analysis was conducted taking into account the calculation of these parameters as normal distribution, which is can be summarized in Table 1.

 Fig. 6The cause–effect diagram for HB.
Table 1

Results analysis of measurements for HB.

#### 3.1.1 GUM procedure to estimate HB uncertainty with and without correlated inputs

To estimate the budget uncertainty in accordance with GUM, sensitivity coefficient should be calculated in accordance with the following equations: (17) (18) (19) The uncertainty budget of HB is summarized in Tables 2 and 3.

Table 2

Uncertainty budget for HB by GUM without correlated inputs.

Table 3

Uncertainty budget for HB by GUM with correlated inputs.

#### 3.1.2 MCS procedure to estimate HB uncertainty and without correlated inputs

10 000 iterations were performed on each parameter contributing the uncertainty budge using equation (13) to estimate the budget uncertainty (see Tab. 4; Fig. 7).

Table 4

Iterations of the input parameters for uncertainty budget of HB by MCS.

 Fig. 7Results of HB by MCS.

#### 3.1.3 Summary of the results of uncertainty budget estimation of HB by MCS

MCS for HB without correlated inputs

Mean value: 100.1 HB.

Expanded uncertainty: 0.67 HB.

MCS for HB with correlated inputs

Mean value: 100.1 HB.

Expanded uncertainty: 0.59 HB.

### 3.2 Procedure to estimate the uncertainty of HV

The detected input sources of uncertainty of HV measurements can be summarizes as shown in Figure 8 and Table 5.

 Fig. 8The cause–effect diagram for HV.
Table 5

Results analysis of Vickers hardness measurements.

#### 3.2.1 GUM procedure to estimate HV uncertainty with and without correlated inputs

To estimate the uncertainty budget of HV sensitivity coefficient should be identified by the following equations (see Tabs. 6 and 7). (20) (21)

Table 6

Uncertainty budget for HV by GUM without correlated inputs.

Table 7

Uncertainty budget for HV by GUM with correlated inputs.

#### 3.2.2 MCS procedure to estimate HV uncertainty with and without correlated inputs

10 000 iterations were performed on each parameter contributing the uncertainty budge using equation (16), to estimate the budget uncertainty (see Tab. 8; Fig. 9).

Table 8

Iterations of the input parameters for uncertainty budget of HV by MCS.

 Fig. 9Result of the Monte Carlo simulation for HV.

#### 3.2.3 Summary of the results of uncertainty budget estimation by MCS

MCS for HV without correlated inputs

Mean value: 401.9 HB.

Expanded uncertainty: ±6.5 HV.

MCS for HV with correlated inputs

Mean value: 401.9 HB.

Expanded uncertainty: ±5.8 HV.

## 4 Discussion

From the previous figures and tables it was noted that the resultant expanded uncertainties (at 95% confidence levels) obtained with the GUM and MCS without correlated inputs for HB were ±0.69 HB, ±0.67 HB and for HV were ±6.7 HV, ±6.5 HV, respectively. The estimated expanded uncertainties with correlated inputs by GUM and MCS were ±0.6 HB, ±0.59 HB and for HV were ±6 HV, ±5.8 HV, respectively. GUM Framework overestimates a little bit the MCS estimated uncertainty. The main cause of this difference is the approximation used by the GUM Framework in estimating the budget uncertainty of the calibration curve produced by least squares regression.

The correlations between inputs have significant effects on the estimated uncertainties. At GUM procedure the estimated uncertainty of HB without correlated inputs was 0.69 HB and 0.6 HB at correlated inputs. For HV the estimated uncertainty without correlated inputs was 6.7 HV and 6 HV at correlated inputs. The same results were obtained in the case of MCS investigation.

Skewness calculation showed small value and hence a symmetrical distribution for the obtained results.

The shape of Kurtosis quantifications showed that the data distribution matches the Gaussian distribution.

Also, it was observed that MCS has features to avoid the limitations and assumptions of the GUM framework. The resulting analysis shows that MCS has many advantages over conventional method (GUM) in uncertainty estimation, especially that of complex measurement systems. MCS is relatively simple to implement; there is no need for complex mathematics related to calculating sensitivity coefficient by partial differentiation and also it was demonstrated that the MCS is relatively compatible with the conventional uncertainty estimation methods of linear systems and systems that have small uncertainties.

## 5 Conclusions

From this research article it was concluded that:

• the expanded uncertainty results estimated with the GUM Framework and the MCS showed no significant differences. In all the cases the estimated uncertainty using the GUM approach slightly overestimated the results obtained with the MCS;

• the correlations between inputs have significant effects on the estimated uncertainties. Thus the correlation between inputs decreases the contribution of these inputs in the budget uncertainty and hence decreases the resultant uncertainty by about 10%, and this value is depending on the correlation coefficient value;

• the result analysis shows that the MCS has numerous advantages over the traditional method (GUM) in the estimation of uncertainty, especially that of complex systems of measurements. There is no need for complex mathematics related to calculating sensitivity coefficient by partial differentiation;

• it was demonstrated that the MCS is relatively compatible with the GUM as a conventional uncertainty estimation methods of linear systems and systems that have small uncertainties.

## References

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Cite this article as: Gouda M. Mahmoud, Riham S. Hegazy, Comparison of GUM and Monte Carlo methods for the uncertainty estimation in hardness measurements, Int. J. Metrol. Qual. Eng. 8, 14 (2017)

## All Tables

Table 1

Results analysis of measurements for HB.

Table 2

Uncertainty budget for HB by GUM without correlated inputs.

Table 3

Uncertainty budget for HB by GUM with correlated inputs.

Table 4

Iterations of the input parameters for uncertainty budget of HB by MCS.

Table 5

Results analysis of Vickers hardness measurements.

Table 6

Uncertainty budget for HV by GUM without correlated inputs.

Table 7

Uncertainty budget for HV by GUM with correlated inputs.

Table 8

Iterations of the input parameters for uncertainty budget of HV by MCS.

## All Figures

 Fig. 1GUM and propagation of uncertainties. In the text
 Fig. 2Schematic to the main idea of MCS. In the text
 Fig. 3The normal distribution, and standard deviation with the confidence level. In the text
 Fig. 4Schematic represents the Brinell hardness test. In the text
 Fig. 5Schematic represents Vickers hardness test. In the text
 Fig. 6The cause–effect diagram for HB. In the text
 Fig. 7Results of HB by MCS. In the text
 Fig. 8The cause–effect diagram for HV. In the text
 Fig. 9Result of the Monte Carlo simulation for HV. In the text

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